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HRID1259512

反应详情

EQUATION

反应方程式

HRID 1259512 的结构方程式

REACTANTS

反应物

3
反应SMILES：II
HCID807

Iodine

I2

反应SMILES：[NH4+].[OH-]
HCID14923

Ammonium hydroxide

H5NO

反应SMILES：COc1c(O)ccc(C=O)c1[N+](=O)[O-]
HCID96959

Benzaldehyde, 4-hydroxy-3-methoxy-2-nitro-

C8H7NO5

PRODUCTS

产物

1
反应SMILES：COc1c(O)ccc(C#N)c1[N+](=O)[O-]
HCID7059265

4-hydroxy-3-methoxy-2-nitrobenzonitrile

C8H6N2O4

AUXILIARIES

试剂、催化剂与溶剂

1
反应SMILES：C1CCOC1
溶剂HCID8028

Tetrahydrofuran

C4H8O

PROCEDURE

实验过程

4-Hydroxy-3-methoxy-2-nitrobenzaldehyde (200 g, 1.01 mol) was dissolved in THF (2.5 L) and then ammonium hydroxide (2.5 L) was added followed by iodine (464 g, 1.8 mol).