HRID128045

反应详情

EQUATION

反应方程式

HRID 128045 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

Reaction of 3-methyl-12-phenyl-1-aza-1,5,9-cyclododecatriene with hydroxylamine hydrochloride, in the presence of hydrochloric acid and water, to 2-methyl-11-phenyl-11-amino-undeca-4,8-dienal-oxime, and hydrogenation of this to give 1-phenyl-10-methyl-1,11-diaminoundecane; b.p. 138°-140° C./1 Pa; nD20 =1.5095.