HRID128280

反应详情

EQUATION

反应方程式

HRID 128280 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

Prepared analogous to Example 1(a) from 3-chloro-6-methyl-benzo[b] thiophene-2-carboxylic acid chloride (m.p.: 124.5°-126° C.) by hydrolysis with aqueous sodium hydroxide solution and subsequent reaction with sodium hydrogen sulfite in the presence of copper-(I)-chloride as a catalyst.