反应详情

A solution of 1-bromodecane in butanone was added dropwise to a stirred refluxing solution of 4-bromo-2-fluorophenol and potasium carbonate. The stirred mixture was heated under reflux for 24 hr. The potassium carbonate was filtered off and the solvent removed. The product was distilled at 130° C. at 0.05 mmHg.

1. temperatureThe stirred mixture was heated
2. temperatureunder reflux for 24 hr
3. filtrationThe potassium carbonate was filtered off
4. customthe solvent removed
5. distillationThe product was distilled at 130° C. at 0.05 mmHg