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HRID130729

反应详情

EQUATION

反应方程式

HRID 130729 的结构方程式

REACTANTS

反应物

3
结构：O=Cc1ccc(O)cc1
HCID126

p-Hydroxybenzaldehyde

C7H6O2

结构：O=C([O-])[O-].[K+].[K+]
HCID11430

Potassium Carbonate

CK2O3

结构：N#Cc1ccc(F)c(F)c1
HCID587203

3,4-Difluorobenzonitrile

C7H3F2N

PRODUCTS

生成物

1
结构：N#Cc1ccc(Oc2ccc(C=O)cc2)c(F)c1
HCID53425670

3-Fluoro-4-(4-formylphenoxy)benzonitrile

C14H8FNO2

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CN(C)C=O
溶剂HCID6228

N,N-Dimethylformamide

C3H7NO

PROCEDURE

实验过程

Basic displacement reaction of 4-hydroxy benzaldehyde and 3,4 difluorobenzonitrile using potassium carbonate in anhydrous DMF at reflux temperatures affords the above compound.

WORKUP

后处理

  1. temperatureat reflux temperatures
  2. customaffords the above compound