huagongshe.com
HRID132803

反应详情

EQUATION

反应方程式

HRID 132803 的结构方程式

REACTANTS

反应物

2
结构：CC(C)(C)OC(=O)OC(=O)OC(C)(C)C
HCID90495

Di-tert-butyl dicarbonate

C10H18O5

结构：CC1(C)OC[C@H]([C@@H](O)CN)O1
HCID59734745

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)(C)OC(=O)NC[C@H](O)[C@H]1COC(C)(C)O1
HCID14249481

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：C1CCOC1
溶剂HCID8028

Tetrahydrofuran

C4H8O

PROCEDURE

实验过程

Aminoalcohol 23 was dissolved in THF and BOC2O was added and stirred for several hrs. The solvent was removed and the product purified using silica gel chromatography.

WORKUP

后处理

  1. customThe solvent was removed
  2. customthe product purified