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HRID1406527

反应详情

EQUATION

反应方程式

HRID 1406527 的结构方程式

REACTANTS

反应物

3
结构：Cc1cnc(N)cc1C
HCID12404013

4,5-Dimethylpyridin-2-amine

C7H10N2

结构：[CH3][Al]([CH3])[CH3]
HCID16682925

Aluminum, trimethyl-

C3H9Al

结构：CCOC(=O)c1cc2nc(Nc3c(Cl)cccc3Cl)n(C)c2cc1F
HCID67229860

未命名化合物

PRODUCTS

生成物

1
结构：Cc1cnc(NC(=O)c2cc3nc(Nc4c(Cl)cccc4Cl)n(C)c3cc2F)cc1C
HCID58562291

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

2
结构：C1CCOC1
溶剂HCID8028

Tetrahydrofuran

C4H8O

结构：CCCCCC
溶剂HCID8058

n-Hexane

C6H14

PROCEDURE

实验过程

Prepared analogously to example 131f from ethyl 2-(2,6-dichlorophenylamino)-6-fluoro-1-methyl-1H-benzimidazole-5-carboxylate, 2 M trimethyl aluminium solution in hexane and 4,5-dimethylpyridin-2-amine in THF.