反应详情

A mixture of compound 3k (1.6 g, 3.9 mmol) and K2CO3 (1.6 g, 12 mmol) in dry THF (30 mL) was stirred at rt overnight. LCMS indicated the total consumption of compound 3k. The reaction mixture was filtered and the filtrate was evaporated in vacuum to give 3l as a white solid (1.1 g, 86% yield).

1. customthe total consumption of compound 3k
2. filtrationThe reaction mixture was filtered
3. customthe filtrate was evaporated in vacuum