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HRID1434524

反应详情

EQUATION

反应方程式

HRID 1434524 的结构方程式

REACTANTS

反应物

3
结构：C[C@H]1C(=O)OC[C@@H]1NC(=O)OCc1ccccc1
HCID13108321

未命名化合物

结构：[CH3][Al]([CH3])[CH3]
HCID16682925

Aluminum, trimethyl-

C3H9Al

结构：Cc1cc(N)ccc1N1CCOCC1=O
HCID23105288

4-(4-Amino-2-methylphenyl)morpholin-3-one

C11H14N2O2

PRODUCTS

生成物

1
结构：Cc1cc(NC(=O)[C@H](C)[C@H](CO)NC(=O)OCc2ccccc2)ccc1N1CCOCC1=O
HCID86605956

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：C1CCOC1
溶剂HCID8028

Tetrahydrofuran

C4H8O

PROCEDURE

实验过程

Prepared analogously to Example 2b from 4-(4-amino-2-methyl-phenyl)-morpholin-3-one and benzyl [(3R,4R)-4-methyl-5-oxo-tetrahydrofuran-3-yl]-carbamate with trimethylaluminium in THF and subsequent purification by reversed-phase chromatography.