Magnesium Stearate → Magnesium Stearate

HRID 1448506Notes

Reaction equation

HRID 1448506 reaction equation
[OH-].[Mg+2:2].[OH-].[OH-].[Ca+2:5].[OH-].[O-2].[Zn+2:8].[C:9]([O-:28])(=[O:27])[CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH3:26].[Mg+2].[C:30]([O-:49])(=[O:48])[CH2:31][CH2:32][CH2:33][CH2:34][CH2:35][CH2:36][CH2:37][CH2:38][CH2:39][CH2:40][CH2:41][CH2:42][CH2:43][CH2:44][CH2:45][CH2:46][CH3:47]>O>[Mg:2].[Ca:5].[Zn:8].[C:9]([O-:28])(=[O:27])[CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH3:26].[Mg+2:2].[C:30]([O-:49])(=[O:48])[CH2:31][CH2:32][CH2:33][CH2:34][CH2:35][CH2:36][CH2:37][CH2:38][CH2:39][CH2:40][CH2:41][CH2:42][CH2:43][CH2:44][CH2:45][CH2:46][CH3:47]

Participants

9

Reactant 4

HCID 11177Magnesium StearateHCID 73981Magnesium HydroxideHCID 3007857Zinc OxideHCID 6093208Calcium Hydroxide

Product 4

HCID 11177Magnesium StearateHCID 23994ZincHCID 5460341CalciumHCID 5462224Magnesium

Reagents, catalysts & solvents 1

HCID 962WaterSolvent2×

Procedure

Aqueous solutions of a group of magnesium, calcium and zinc salts were prepared by mixing 0.06 moles of the organic acid with 0.033 moles of either magnesium hydroxide, calcium hydroxide or zinc oxide in 780 g of water, then heating the mixture to the reflux temperature with stirring for three hours followed by cooling to room temperature and filtering. A magnesium stearate solution was prepared by heating excess commercial magnesium stearate in water with stirring for four hours followed by cooling and filtering. The metal content of each solution was estimated by atomic absorption.

Workup

  1. temperatureheating the mixture to the reflux temperature
  2. filtrationfiltering
  3. stirringwith stirring for four hours
  4. temperatureby cooling
  5. filtrationfiltering
  6. customThe metal content of each solution was estimated by atomic absorption

Sources & evidence

ORD record
ord-932541298c3a4f17be3624e00a3aece1
Source dataset
uspto-grants-1979_12
Patent number
US04180620

Reaction notes

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