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HRID1457916

反应详情

EQUATION

反应方程式

HRID 1457916 的结构方程式

REACTANTS

反应物

3
结构：BrCc1ccccc1
HCID7498

alpha-Bromotoluene

C7H7Br

结构：O=C([O-])[O-].[K+].[K+]
HCID11430

Potassium Carbonate

CK2O3

结构：COC(=O)c1ccc(O)c(C(C)=O)c1
HCID12332833

Methyl 3-acetyl-4-hydroxybenzoate

C10H10O4

PRODUCTS

生成物

1
结构：COC(=O)c1ccc(OCc2ccccc2)c(C(C)=O)c1
HCID22101033

Methyl 3-acetyl-4-(benzyloxy)benzoate

C17H16O4

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CN(C)C=O
溶剂HCID6228

N,N-Dimethylformamide

C3H7NO

PROCEDURE

实验过程

1.0 eq. of methyl 3-acetyl-4-hydroxybenzoate was reacted with 1.1 eq. each of K2CO3 and benzyl bromide in absolute DMF to form methyl 3-acetyl-4-benzyloxybenzoate. Colorless crystals, mp 68°-72° C.