HRID1470792
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
This reaction is carried out in the same manner as the reaction in example 4. The difference is that 3-methyl-4-chloride-5-phenyl-2(5H)— furanone (42.0 mg, 0.2 mmol), methoxyphenyl boronic acid (46.5 mg, 97%, 0.3 mmol), palladium acetate (2.3 mg, 0.01 mmol), dicyclohexyl(2,4,6-trimethoxyphenyl)phosphine (7.3 mg, 0.02 mmol), potassium carbonate (82.3 mg, 0.6 mmol) are reacted in 1 mL of toluene at 110° C. for 35 minutes and 3-methyl-4-(methoxyphenyl)-5-phenyl-2(5H)— furanone is obtained. The yield is 100%.
WORKUP
后处理
- customThis reaction is carried out in the same manner as the reaction in example 4