N,N-diethyl-3-fluorobenzamide → HCID 139592774, compound

HRID 1490674Notes

Reaction equation

HRID 1490674 reaction equation
CCN(CC)C(=O)c1cccc(F)c1>C1=CCCC=CCC1.C1=CCCC=CCC1.C1CCOC1.CC1(C)OB(B2OC(C)(C)C(C)(C)O2)OC1(C)C.COc1ccccn1.C[OH2+].C[OH2+].[Ir].[Ir]>CCN(CC)C(=O)c1ccc(B2OC(C)(C)C(C)(C)O2)c(F)c1

Participants

6

Reactant 1

HCID 963334N,N-diethyl-3-fluorobenzamide

Product 1

HCID 139592774HCID 139592774, compoundYield 0%

Reagents, catalysts & solvents 4

HCID 742012-MethoxypyridineReagentHCID 2733548Bis(pinacolato)diboraneReagentHCID 76001521Bis(1,5-cyclooctadiene)dimethoxydiiridiumCatalystHCID 8028TetrahydrofuranSolvent

Conditions

Temperature
80 °C

Sources & evidence

ORD record
ord-39fe8bf34c1f4365bfdc9e1258bd1cdb
Source dataset
Borylation dataset from Roche

Reaction notes

Loading…