Triethylamine → HCID 118380275, compound

HRID 1504569Notes

Reaction equation

HRID 1504569 reaction equation
[C:1]([N:4]([CH2:8][CH2:9][OH:10])[CH2:5][CH2:6][OH:7])(=[O:3])[CH3:2].C(N(CC)CC)C.Cl[C:19](Cl)([O:21]C(=O)OC(Cl)(Cl)Cl)Cl>C1COCC1>[C:1]([N:4]1[CH2:8][CH2:9][O:10][C:19](=[O:21])[O:7][CH2:6][CH2:5]1)(=[O:3])[CH3:2]

Participants

5

Reactant 3

HCID 8471TriethylamineHCID 94429TriphosgeneHCID 9793833N,N-Bis(2-hydroxyethyl)acetamide

Product 1

HCID 118380275HCID 118380275, compound

Reagents, catalysts & solvents 1

HCID 8028TetrahydrofuranSolvent

Procedure

The procedure of Example 1 was followed using N-acetyl diethanolamine (12.3 g, 83.9 mmol), triethylamine (24.0 mL, 167.8 mmol), dry THF (600 mL) and triphosgene (8.3 g, 28.8 mmol). The filtrate was concentrated yielding only oligomeric compounds.

Workup

  1. concentrationThe filtrate was concentrated
  2. customyielding only oligomeric compounds

Sources & evidence

ORD record
ord-1caea859d1c7485c876f6d67cdecfe36
Source dataset
uspto-grants-2015_12
Patent number
US09215876B2

Reaction notes

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