huagongshe.com
HRID15766

反应详情

EQUATION

反应方程式

HRID 15766 的结构方程式

REACTANTS

反应物

6
结构：c1cn[nH]c1
HCID1048

Pyrazole

C3H4N2

结构：NN.O
HCID24654

Hydrazine hydrate (1:1)

H6N2O

结构：COC(OC)N(C)C
HCID78373

Methanamine, 1,1-dimethoxy-N,N-dimethyl-

C5H13NO2

结构：Cl.O=S(=O)(Cl)c1ccccn1
HCID13791306

Pyridine-2-sulfonyl chloride--hydrogen chloride (1/1)

C5H5Cl2NO2S

结构：CC[C@@H]1CC2(C[C@H](CC)N1)OCCO2
HCID59342374

未命名化合物

结构：CCC1CC(=O)CC(CC)N1S(=O)(=O)c1ccccn1
HCID68501382

未命名化合物

PRODUCTS

生成物

1
结构：CC[C@@H]1Cc2[nH]ncc2[C@H](CC)N1S(=O)(=O)c1ccccn1
HCID68495820

未命名化合物

PROCEDURE

实验过程

Prepared by treatment of 2,6-diethyl-1-(pyridin-2-ylsulfonyl)piperidin-4-one, which was prepared by sulfonylation of compound 126 using pyridine-2-sulfonyl chloride hydrochloride followed by deprotection as shown in Example 17, with DMF-DMA followed by pyrazole formation using hydrazine hydrate as shown in Example 15,