huagongshe.com
HRID1580300

反应详情

EQUATION

反应方程式

HRID 1580300 的结构方程式

REACTANTS

反应物

3
结构：OCCCl
HCID34

2-Chloroethanol

C2H5ClO

结构：CSc1ccccc1O
HCID61261

Phenol, 2-(methylthio)-

C7H8OS

结构：CC[O-].[Na+]
HCID2723922

Ethanol, sodium salt

C2H5NaO

PRODUCTS

生成物

1
结构：CSc1ccccc1OCCO
HCID22036270

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCO
溶剂HCID702

Ethanol

C2H6O

PROCEDURE

实验过程

o-Hydroxythioanisole (14.1 g., 0.1 mole) is dissolved in sodium ethoxide (6.8 g., 0.1 mole) in absolute ethanol (100 ml.) and stirred as β-hydroxyethyl chloride (8.1 g., 0.1 mole) is added. The reaction mixture is refluxed for 2 hours and cooled. The o-(β-hydroxyethoxy)-thioanisole is extracted.

WORKUP

后处理

  1. additionis added
  2. temperatureThe reaction mixture is refluxed for 2 hours
  3. temperaturecooled
  4. extractionThe o-(β-hydroxyethoxy)-thioanisole is extracted