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HRID1591076

反应详情

EQUATION

反应方程式

HRID 1591076 的结构方程式

REACTANTS

反应物

4
结构：OO
HCID784

Hydrogen peroxide

H2O2

结构：O
HCID962

Water

H2O

结构：O=C([O-])[O-].[K+].[K+]
HCID11430

Potassium Carbonate

CK2O3

结构：N#Cc1ccc2c(c1)CCC=C2n1ccnc1
HCID9837392

未命名化合物

PRODUCTS

生成物

1
结构：NC(=O)c1ccc2c(c1)CCC=C2n1ccnc1
HCID19766492

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

2
结构：CS(C)=O
溶剂HCID679

Dimethyl sulfoxide

C2H6OS

结构：ClCCl
溶剂HCID6344

Dichloromethane

CH2Cl2

PROCEDURE

实验过程

Potassium carbonate and 30% aqueous H2O2 solution are added several times, within a period of 24 hours, to 6-cyano-1-(1-imidazolyl)-3,4-dihydronaphthalene (Example 1) in DMSO and CH2Cl2. Finally, water is added and the solid is filtered off, yielding the title compound.

WORKUP

后处理

  1. filtrationthe solid is filtered off