Hydrogen Peroxide → Hydrogen Peroxide

HRID 1633394Notes

Reaction equation

HRID 1633394 reaction equation
[OH:1][CH2:2][C:3]1[CH:10]=[CH:9][C:6]([O:7][CH3:8])=[CH:5][CH:4]=1.[OH:11][OH:12]>CC(C)=O>[CH3:8][O:7][C:6]1[CH:5]=[CH:4][C:3]([CH:2]=[O:1])=[CH:10][CH:9]=1.[OH:11][OH:12]

Participants

5

Reactant 2

HCID 784Hydrogen PeroxideHCID 77384-Methoxybenzyl alcohol

Product 2

HCID 784Hydrogen PeroxideYield 94%HCID 312444-Methoxybenzaldehyde

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

11.15 g of anise alcohol, 39 g of acetone, 2 g of catalyst and 2 cc of 36% w/v aqueous hydrogen peroxide are placed in the glass flask. Operating at 80° C., 3 g of anisaldehyde are obtained (H2O2 yield 94%).

Workup

  1. customOperating at 80° C.

Sources & evidence

ORD record
ord-a87abb6c50f24ccb93d32ff09963d551
Source dataset
uspto-grants-1984_10
Patent number
US04480135

Reaction notes

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