HRID1639078

反应详情

EQUATION

反应方程式

HRID 1639078 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

This compound was prepared according to the procedure of Example 6. A mixture of 3.6 g (0.02 mole) of 1-(4-fluorophenyl)piperazine, 4.0 g (0.02 mole) of 4-chloro-1-phenoxy 2-butanol and 5.3 g (0.05 mole) of anhydrous sodium carbonate in 100 ml of 1-butanol gave 5.1 g (74%) of offwhite powder, m.p. 97°-99° C. Recrystallizing solvent used was isopropyl alcohol.

WORKUP

后处理

  1. customThis compound was prepared
  2. customgave 5.1 g (74%) of offwhite powder, m.p. 97°-99° C