HRID1648673

反应详情

EQUATION

反应方程式

HRID 1648673 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

N,N'-Bis-(4-phenoxyphenyl)-2,6-pyridine dicarboxamide was prepared from p-phenoxyaniline and 2,6-pyridine dicarboxylic acid dichloride. The amide (8.0248 g, 0.016 moles) was polymerized with isophthaloyl chloride (3.2484 g, 0.016) using the procedure of Example 27. The amounts of aluminum chloride, DMF and DCE used were 21.33 g (0.160 moles), 4.71 mL (0.061 mol) and 100 mL, respectively. The off-white fibrous polymer which was obtained had the repeat unit ##STR46##

WORKUP

后处理

  1. customThe off-white fibrous polymer which was obtained