Benzoic Acid → HCID 86738142, compound

HRID 1659440Notes

Reaction equation

HRID 1659440 reaction equation
[Si:1]([O-:5])([O-:4])([O-:3])[O-:2].[Na+:6].[Na+].[Na+].[Na+].[Na].[C:11](O)(=O)[C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1.S(OOS([O-])(=O)=O)([O-])(=O)=O.[K+].[K+].[C:32](OOC(=O)C1C=CC=CC=1)(=O)C1C=CC=CC=1>>[Si:1]([O-:5])([O-:4])([O-:3])[O-:2].[Na+:6].[Na+:6].[Na+:6].[Na+:6].[CH2:32]=[CH:11][C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1

Participants

6

Reactant 5

HCID 243Benzoic AcidHCID 7187Benzoyl PeroxideHCID 24412Potassium PersulfateHCID 26051Sodium orthosilicateHCID 5360545Sodium

Product 1

HCID 86738142HCID 86738142, compound

Procedure

About 30 parts by weight of an aqueous sodium silicate solution containing 14.7% Na2O and 29.4% SiO2 by weight, 20 parts by weight of styrenes, 0.5 parts by weight of the sodium salt of ricinoleic sulphonates and 1 part by weight of benzoic acid are thoroughly mixed and emulsified; then 0.1 part by weight of potassium persulfate, 0.01 part by weight of ferric sulfate and 0.1 part by weight of benzoyl peroxide is added to the emulsion and thoroughly mixed at ambient temperature (24° C.) and pressure. The mixture is polymerized in 1 to 24 hours thereby producing a poly(sodium silicate-styrene) copolymer emulsion.

Workup

  1. additionare thoroughly mixed
  2. additionthoroughly mixed at ambient temperature (24° C.) and pressure
  3. customThe mixture is polymerized in 1 to 24 hours

Sources & evidence

ORD record
ord-043bc59719d84cea966a3f1a2d554f63
Source dataset
uspto-grants-1981_12
Patent number
US04303768

Reaction notes

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