Dimethylformamide → Azide

HRID 168878Notes

Reaction equation

HRID 168878 reaction equation
[CH3:25][CH2:26][N:27]([CH2:28][CH3:29])[CH2:30][CH3:31].[CH3:49][N:50]([CH3:51])[CH:52]=[O:53].[Cl:1][c:2]1[c:3](-[n:13]2[n:14][c:15]([C:22](=[S:23])[OH:24])[c:16]([C:18]([F:19])([F:20])[F:21])[cH:17]2)[c:4]([Cl:12])[cH:5][c:6]([C:8]([F:9])([F:10])[F:11])[cH:7]1.[c:32]1([P:33]([c:34]2[cH:35][cH:36][cH:37][cH:38][cH:39]2)(=[O:40])[N:46]=[N+:47]=[N-:48])[cH:41][cH:42][cH:43][cH:44][cH:45]1>>[Cl:1][c:2]1[c:3](-[n:13]2[n:14][c:15]([C:22](=[S:23])[OH:24])[c:16]([C:18]([F:19])([F:20])[F:21])[cH:17]2)[c:4]([Cl:12])[cH:5][c:6]([C:8]([F:9])([F:10])[F:11])[cH:7]1.[N-:46]=[N+:47]=[N-:48]

Participants

6

Reactant 4

HCID 6228DimethylformamideHCID 8471TriethylamineHCID 199401P,P-Diphenylphosphinic azideHCID 178526154HCID 178526154, compound

Product 2

HCID 33558AzideHCID 178526154HCID 178526154, compound

Sources & evidence

ORD record
ord-a8507b1d3c5342869498e88f87c69ade
Source dataset
Training data from https://doi.org/10.1039/C8SC04228D (9/10)

Reaction notes

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