huagongshe.com
HRID1701837

反应详情

EQUATION

反应方程式

HRID 1701837 的结构方程式

REACTANTS

反应物

3
结构：NC(=O)CI
HCID3727

Iodoacetamide

C2H4INO

结构：[H-].[Na+]
HCID24758

Sodium hydride

HNa

结构：O=C(Nc1ncc([N+](=O)[O-])s1)c1cccc([N+](=O)[O-])c1
HCID298930

MLS000756380

C10H6N4O5S

PRODUCTS

生成物

1
结构：NC(=O)Cn1cc([N+](=O)[O-])sc1=NC(=O)c1cccc([N+](=O)[O-])c1
HCID3061827

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CN(C)C=O
溶剂HCID6228

N,N-Dimethylformamide

C3H7NO

PROCEDURE

实验过程

By following the procedure of Example 5, but using a dispersion of sodium hydride (2.1 g 60% w/w) in mineral oil, 3-nitro-N-(5-nitro-2-thiazolyl)benzamide (11.8 g), N,N-dimethylformamide (100 ml) and 2-iodoacetamide (11.1 g), there was obtained 2-[(3-nitrobenzoyl)imino]-5-nitro-4-thiazoline-3-acetamide, m.pt 251°-252°, after recrystallization from pyridine.