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HRID1726107

反应详情

EQUATION

反应方程式

HRID 1726107 的结构方程式

REACTANTS

反应物

3
结构：O=[N+]([O-])c1ccc(O)cc1
HCID980

4-Nitrophenol

C6H5NO3

结构：[H-].[Na+]
HCID24758

Sodium hydride

HNa

结构：CP(=S)(Cl)Cl
HCID61195

Phosphonothioic dichloride, methyl-

CH3Cl2PS

PRODUCTS

生成物

1
结构：CP(=S)(Oc1ccc([N+](=O)[O-])cc1)Oc1ccc([N+](=O)[O-])cc1
HCID11416910

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：C1CCOC1
溶剂HCID8028

Tetrahydrofuran

C4H8O

PROCEDURE

实验过程

The methylphosphonothioic acid O,O-bis-(4-nitrophenyl)ester intermediate is prepared according to procedure E using 536 mg of methylphosphonothioic dichloride, 345 mg of sodium hydride (50% in oil), 1 g of p-nitrophenol and 10 ml of tetrahydrofuran. 1.19 g of expected product are collected.

WORKUP

后处理

  1. custom1.19 g of expected product are collected