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HRID1755827

反应详情

EQUATION

反应方程式

HRID 1755827 的结构方程式

REACTANTS

反应物

3
结构：CCN(CC)CC
HCID8471

Triethylamine

C6H15N

结构：O=C(Cl)OCc1ccccc1
HCID10387

Benzyl chloroformate

C8H7ClO2

结构：C=CCN[C@H](C)C(=O)OC(C)(C)C
HCID54332184

未命名化合物

PRODUCTS

生成物

1
结构：C=CCN(C(=O)OCc1ccccc1)[C@H](C)C(=O)OC(C)(C)C
HCID54427579

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：ClCCl
溶剂HCID6344

Dichloromethane

CH2Cl2

PROCEDURE

实验过程

N-Allyl-D-alanine t-butyl ester (69) is treated with 1.1 equivalents of benzyl chloroformate and 1.1 equivalents of triethylamine in methylene chloride at room temperature overnight. After evaporation of solvent, the product is purified by silica gel chromatography to give (70).

WORKUP

后处理

  1. customAfter evaporation of solvent
  2. customthe product is purified by silica gel chromatography