Methacrylamide → HCID 15084876, compound

HRID 1763088Notes

Reaction equation

HRID 1763088 reaction equation
[OH-].[K+].[C:3]([NH2:8])(=[O:7])[C:4]([CH3:6])=[CH2:5].Cl[CH2:10][CH2:11][C:12]#[N:13].[CH:14]1C2NC3C(=CC=CC=3)SC=2C=CC=1>CN(C)C=O>[C:12]([CH2:11][CH2:10][N:8]([CH3:14])[C:3](=[O:7])[C:4]([CH3:6])=[CH2:5])#[N:13]

Participants

6

Reactant 4

HCID 6595MethacrylamideHCID 7108PhenothiazineHCID 109633-ChloropropionitrileHCID 14797Potassium Hydroxide

Product 1

HCID 15084876HCID 15084876, compound

Reagents, catalysts & solvents 1

HCID 6228DimethylformamideSolvent

Procedure

To 150 ml of N,N-dimethylformamide, were added 28 g of potassium hydroxide, 17 g of methacrylamide, 23 g of 3-chloropropionitrile and 0.05 g of phenothiazine. A reaction was carried out at 40° C. for 3 hours with stirring.

Sources & evidence

ORD record
ord-a04e22ce01c3495393ed1370ff0ffb44
Source dataset
uspto-grants-1989_05
Patent number
US04835312

Reaction notes

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