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HRID1767956

反应详情

EQUATION

反应方程式

HRID 1767956 的结构方程式

REACTANTS

反应物

4
结构：c1ccc(P(c2ccccc2)c2ccccc2)cc1
HCID11776

Triphenylphosphine

C18H15P

结构：CC(C)(C)OC(=O)N=NC(=O)OC(C)(C)C
HCID97268

Di-tert-butyl azodicarboxylate

C10H18N2O4

结构：Cc1sc(-c2ccccc2)nc1CCO
HCID2760018

2-(5-Methyl-2-phenyl-1,3-thiazol-4-yl)ethan-1-ol

C12H13NOS

结构：CC(C)(C)OC(=O)Cn1ccc2ccc(O)cc21
HCID69283069

tert-Butyl (6-hydroxy-1H-indol-1-yl)acetate

C14H17NO3

PRODUCTS

生成物

1
结构：Cc1sc(-c2ccccc2)nc1CCOc1ccc2ccn(CC(=O)OC(C)(C)C)c2c1
HCID69280517

未命名化合物

PROCEDURE

实验过程

In analogy to the procedure described in example 3 c], (6-hydroxy-indol-1-yl)-acetic acid tert-butyl ester (example 6 b]) was reacted with 2-(5-methyl-2-phenyl-thiazol-4-yl)-ethanol in the presence of triphenylphosphine and di-tert-butyl azodicarboxylate to yield {6-[2-(5-methyl-2-phenyl-thiazol-4-yl)-ethoxy]-indol-1-yl}-acetic acid tert-butyl ester as yellow oil.