huagongshe.com
HRID1775932

反应详情

EQUATION

反应方程式

HRID 1775932 的结构方程式

REACTANTS

反应物

10
结构：C=O
HCID712

Formaldehyde

CH2O

结构：O=C(O)C(F)(F)F
HCID6422

未命名化合物

结构：CCOC(=O)CBr
HCID7748

Ethyl bromoacetate

C4H7BrO2

结构：OC1CCCCC1
HCID7966

Cyclohexanol

C6H12O

结构：Cc1ccc(NN)cc1.Cl
HCID12504

Hydrazine, (4-methylphenyl)-, hydrochloride (1:1)

C7H11ClN2

结构：CCN=C=NCCCN(C)C
HCID15908

1-Ethyl-3-(3'-dimethylaminopropyl)carbodiimide

C8H17N3

结构：CCOC(CCCNC)OCC
HCID13994547

4,4-Diethoxy-N-methylbutan-1-amine

C9H21NO2

结构：Cc1ccc2c(c1)c1c(n2CC(=O)O)CN(C)CC1
HCID44242645

未命名化合物

结构：CCOC(=O)CN(N)c1ccc(C)cc1
HCID57930412

未命名化合物

结构：CCOC(=O)Cn1cc(CCNC)c2cc(C)ccc21
HCID57930443

未命名化合物

PRODUCTS

生成物

1
结构：Cc1ccc2c(c1)c1c(n2CC(=O)OC2CCCCC2)CN(C)CC1
HCID57930424

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

4
结构：CC#N
溶剂HCID6342

Acetonitrile

C2H3N

结构：CCN(CC)CC
溶剂HCID8471

Triethylamine

C6H15N

结构：[Na+].[OH-]
溶剂HCID14798

Sodium Hydroxide

HNaO

结构：CCOC(=O)Cn1c2c(c3cc(C)ccc31)CCN(C)C2
溶剂HCID57930374

未命名化合物

PROCEDURE

实验过程

The title compound is prepared by following General Methods 1, 3, 4, 5 and 6 by using p-tolylhydrazine hydrochloride, ethyl bromoacetate, and triethylamine (General Method 1), ethyl 2-(1-(4-methylphenyl)hydrazinyl)acetate and 4,4-diethoxy-N-methylbutan-1-amine (General Method 3), ethyl 2-(5-methyl-3-(2-(methylamino)ethyl)-1H-indol-1-yl)acetate, formaldehyde and TFA in acetonitrile (General Method 4), ethyl 2-(6-methyl-1,2,3,4-tetrahydro-2-methylpyrido[3,4-b]indol-9-yl)acetate and NaOH (General Method 5), and 2-(6-methyl-1,2,3,4-tetrahydro-2-methylpyrido[3,4-b]indol-9-yl)acetic acid, cyclohexanol and EDCI (General Method 6).