反应详情

温度

60 °C

A mixture of 0.7 g of 4-benzyloxy-3-methoxymethoxypyridine and 1N hydrochloric acid was stirred for 2 hours at 60° C. The mixture was poured into saturated aqueous sodium bicarbonate solution, extracted with ethyl acetate. The organic layer is washed with saturated saline, dried over anhydrous magnesium sulfate, concentrated to obtain 0.547 g of 4-benzyloxy-3-hydroxypyridine.

1. extractionextracted with ethyl acetate
2. washThe organic layer is washed with saturated saline
3. dry with materialdried over anhydrous magnesium sulfate
4. concentrationconcentrated