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HRID1871398

反应详情

EQUATION

反应方程式

HRID 1871398 的结构方程式

REACTANTS

反应物

2
结构：Cc1ccc(S(=O)(=O)O)cc1
HCID6101

4-Methylbenzenesulfonic acid

C7H8O3S

结构：COc1ccc(C2=NN(c3ccc(C(=O)O)cc3)C(=O)[C@H]3CC=CC[C@@H]23)cc1OC
HCID86755612

未命名化合物

PRODUCTS

生成物

1
结构：CCCOC(=O)c1ccc(N2N=C(c3ccc(OC)c(OC)c3)[C@@H]3CC=CC[C@@H]3C2=O)cc1
HCID131721941

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCCO
溶剂HCID1031

1-Propanol

C3H8O

PROCEDURE

实验过程

A solution of 1 g of compound 67 and 1 g of p-toluenesulfonic acid in 100 ml of 1-propanol was refluxed for 18 h. After evaporating the solvent, the title compound was crystallized from methanol. M.p. 100°-101° C.

WORKUP

后处理

  1. customAfter evaporating the solvent
  2. customthe title compound was crystallized from methanol