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HRID1902147

反应详情

EQUATION

反应方程式

HRID 1902147 的结构方程式

REACTANTS

反应物

3
结构：O=C(O)C(F)(F)F
HCID6422

未命名化合物

结构：COc1ccccc1
HCID7519

Anisole

C7H8O

结构：CC(C)(C)OC(=O)N1CCC2(CC1)CC(=O)C1CC=CC=C12
HCID19030439

未命名化合物

PRODUCTS

生成物

1
结构：NC(=O)C(F)(F)F.O=C1CC2(CCNCC2)c2ccccc21
HCID18467060

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：ClCCl
溶剂HCID6344

Dichloromethane

CH2Cl2

PROCEDURE

实验过程

A solution of the intermediate from Step A in a 1:1:0.5 mixture of trifluoroacetic acid, dichloromethane and anisole was stirred for 1 hour and then concentrated and azeotroped from toluene to give the title compound.

WORKUP

后处理

  1. concentrationconcentrated
  2. customazeotroped from toluene