HRID1906935

反应详情

EQUATION

反应方程式

HRID 1906935 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

This compound was prepared in the same manner as described in Example 7 using sodium hydride (0.036 g, 50% in mineral oil; 0.90 mmol), dimethylformamide (5 ml), 3-phenylsulfinylindole (0.200 g, 0.82 mmol) and benzyl bromide (0.11 ml, 0.154 g, 0.90 mmol). Crystallization of the crude product from dichloromethane-hexane gave the title compound. M.P.-148°-149° (dichloromethane-hexane).

WORKUP

后处理

  1. customThis compound was prepared in the same manner
  2. customCrystallization of the crude product from dichloromethane-hexane