1-Butanol → HCID 13828760, compound

HRID 1946219Notes

Reaction equation

HRID 1946219 reaction equation
[Mg:1].C(O)CCC.[F:7][C:8]([F:13])([F:12])[C:9]([OH:11])=[O:10]>C(O)(C)C>[F:7][C:8]([F:13])([F:12])[C:9]([O-:11])=[O:10].[Mg+2:1].[F:7][C:8]([F:13])([F:12])[C:9]([O-:11])=[O:10]

Participants

5

Reactant 3

HCID 2631-ButanolHCID 6422Trifluoroacetic acidHCID 5462224Magnesium3×

Product 1

HCID 13828760HCID 13828760, compound

Reagents, catalysts & solvents 1

HCID 3776IsopropanolSolvent

Procedure

A soda lime glass substrate having a diameter of 30 mm and a thickness of 1 mm was ultrasonically cleaned in isopropyl alcohol and was then dried, whereby a glass substrate for coating was prepared. To one mass part of powdery magnesium available from Kishida Chemical Co., Ltd. and 18 mass parts of 1-butanol, 25 mass parts of trifluoroacetic acid (CF3COOH) was gradually added, whereby magnesium was completely dissolved. A solution containing completely dissolved magnesium was filtered and was then vacuum-dried, whereby magnesium trifluoroacetate was obtained.

Workup

  1. customwas then dried
  2. customwhereby a glass substrate for coating was prepared
  3. filtrationwas filtered
  4. customwas then vacuum-dried

Sources & evidence

ORD record
ord-2023c2ef4349495e8cab6317a1ef8119
Source dataset
uspto-grants-2013_03
Patent number
US08399069B2

Reaction notes

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