反应详情

Ethylacetoacetate (10 g) and 4-(trifluoromethyl) aniline (12.38 g) in xylene (250 ml) was refluxed for 48 hours. Reaction mixture was concentrated and purified by column chromatography to give pure (9.7 g).

1. customReaction mixture
2. concentrationwas concentrated
3. custompurified by column chromatography
4. customto give pure (9.7 g)