Hydroxylamine → HCID 20217861, compound

HRID 1981784Notes

Reaction equation

HRID 1981784 reaction equation
BrC1CCC(=O)CC1.[Na].[C:10]1([S:16][C:17]2[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=2)[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=1.[NH2:23][OH:24]>CN(C)C=O>[C:17]1([S:16][CH:10]2[CH2:11][CH2:12][C:13](=[N:23][OH:24])[CH2:14][CH2:15]2)[CH:18]=[CH:19][CH:20]=[CH:21][CH:22]=1

Participants

6

Reactant 4

HCID 787HydroxylamineHCID 8766Diphenyl sulfideHCID 5360545SodiumHCID 114010884-Bromocyclohexan-1-one

Product 1

HCID 20217861HCID 20217861, compound

Reagents, catalysts & solvents 1

HCID 6228DimethylformamideSolvent

Procedure

The title compound is prepared by reacting 4-bromocyclohexanone with the sodium salt of phenyl sulfide in dimethylformamide followed by reacting with hydroxylamine.

Sources & evidence

ORD record
ord-11b72d82f23a4c85a5a578035851ec4e
Source dataset
uspto-grants-1986_06
Patent number
US04593102

Reaction notes

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