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HRID2052813

反应详情

EQUATION

反应方程式

HRID 2052813 的结构方程式

REACTANTS

反应物

3
结构：O=C([O-])[O-].[K+].[K+]
HCID11430

Potassium Carbonate

CK2O3

结构：O=C(CCBr)c1ccccc1
HCID122432

3-Bromo-1-phenylpropan-1-one

C9H9BrO

结构：Cl.Cl.O=C(CN1CCNCC1)c1ccccc1
HCID23080512

1-Phenyl-2-(piperazin-1-yl)ethan-1-one--hydrogen chloride (1/2)

C12H18Cl2N2O

PRODUCTS

生成物

1
结构：CC(C(=O)c1ccccc1)N1CCN(CC(=O)c2ccccc2)CC1.Cl.Cl
HCID69223708

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CN(C)C=O
溶剂HCID6228

N,N-Dimethylformamide

C3H7NO

PROCEDURE

实验过程

A mixture of 3-bromo-1-phenylpropan-1-one (1.5 g, 8.9 mmol), N-phenacyl piperazine dihydrochloride (2.05 g, 7.4 mmol) and K2CO3 (21.75 mmol) in 30 ml of DMF was treated according to the general preparation 2 to give compound (IV-13), 0.64 g (76%), mp 204-205° C., M+ 336.

WORKUP

后处理

  1. additionwas treated
  2. customaccording to the general preparation 2
  3. customto give compound (IV-13), 0.64 g (76%), mp 204-205° C., M+ 336