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HRID2058641

反应详情

EQUATION

反应方程式

HRID 2058641 的结构方程式

REACTANTS

反应物

3
反应SMILES：O=C1c2ccccc2C(=O)C1(O)O
HCID10236

Ninhydrin

C9H6O4

反应SMILES：CC(=O)O.CCCCO.O
HCID22056973

未命名化合物

反应SMILES：N=C(N)NCCC[C@H](NC(=O)[C@@H]1CCCN1C(=O)[C@H](N)Cc1ccccc1)C(=O)CCl
HCID178512868

未命名化合物

PRODUCTS

产物

1
反应SMILES：N[C@@H](Cc1ccccc1)C(=O)O
HCID6140

L-Phenylalanine

C9H11NO2

AUXILIARIES

试剂、催化剂与溶剂

1
反应SMILES：Cl
溶剂HCID313

Hydrochloric Acid

ClH

PROCEDURE

实验过程

Thin layer chromatography on silica gel plates (Merck) with butanol:acetic acid:water (4:1:1) indicated a single spot, Rf 0.37, by uv and by ninhydrin and Sakaguchi stains. Amino acid analysis of the D-Phe-Pro-ArgCH2Cl. 2HCl following hydrolysis in 2 ml of 6.0 N HCl for 24 hr. at 110° C. gave Phe=0.98 and Pro=1.00.