Potassium Acetate → HCID 68123361, compound

HRID 2072328Notes

Reaction equation

HRID 2072328 reaction equation
[CH3:1][N:2]1[C:11]2[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=2)[CH:5]([C:12]2[CH:23]=[CH:22][C:15]([O:16][C:17]([CH3:21])([CH3:20])[CH2:18]Br)=[CH:14][CH:13]=2)[CH2:4][CH2:3]1.[C:24]([O-:27])(=[O:26])[CH3:25].[K+]>CN(C=O)C>[C:24]([O:27][CH2:18][C:17]([O:16][C:15]1[CH:22]=[CH:23][C:12]([CH:5]2[C:6]3[C:11](=[CH:10][CH:9]=[CH:8][CH:7]=3)[N:2]([CH3:1])[CH2:3][CH2:4]2)=[CH:13][CH:14]=1)([CH3:21])[CH3:20])(=[O:26])[CH3:25]

Participants

4

Reactant 2

HCID 517044Potassium AcetateHCID 21408053HCID 21408053, compound

Product 1

HCID 68123361HCID 68123361, compound

Reagents, catalysts & solvents 1

HCID 6228DimethylformamideSolvent

Conditions

Temperature
60 °C

Procedure

3 g. of 2-[4-(1-methyl-1,2,3,4-tetrahydro-4-quinolyl)-phenoxy]-2-methyl-propyl bromide are dissolved in 20 ml. of DMF, 3 g. of anhydrous potassium acetate are added and the mixture is stirred for 3 hours at 60° C. Working up in the usual manner gives 2-[4-(1-methyl-1,2,3,4-tetrahydro-4-quinolyl)-phenoxy]-2-methyl-propyl acetate.

Sources & evidence

ORD record
ord-9080146a95dc43b3a5dc0afb536a8a99
Source dataset
uspto-grants-1977_09
Patent number
US04051173

Reaction notes

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