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HRID20802

反应详情

EQUATION

反应方程式

HRID 20802 的结构方程式

REACTANTS

反应物

4
结构：CCC(C)=O
HCID6569

Methyl ethyl ketone

C4H8O

结构：[C-]#N.[K+]
HCID9032

Potassium cyanide

CKN

结构：C1CCNC1
HCID31268

Pyrrolidine

C4H9N

结构：CC(C)(C#N)N1CCCC1
HCID12570647

2-Methyl-2-(pyrrolidin-1-yl)propanenitrile

C8H14N2

PRODUCTS

生成物

1
结构：CCC(C)(C#N)N1CCCC1
HCID43802838

未命名化合物

收率 63%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：O
溶剂HCID962

Water

H2O

PROCEDURE

实验过程

The title compound (9.6 g, 63%) was prepared from pyrrolidine (8.35 ml, 0.1 mol), 2-butanone (8.96 g, 0.1 mol) and potassium cyanide (6.51 g, 0.1 mol) in water (50 ml) in a similar manner to that described in D4. 1H NMR (CDCl3) δ: 1.06 (3H, t, J=7.2 Hz), 1.45 (3H, s), 1.66-1.93 (6H, m), 2.70-2.75 (4H, m).