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HRID20804

反应详情

EQUATION

反应方程式

HRID 20804 的结构方程式

REACTANTS

反应物

4
结构：CCC(C)=O
HCID6569

Methyl ethyl ketone

C4H8O

结构：[C-]#N.[K+]
HCID9032

Potassium cyanide

CKN

结构：CNC.Cl
HCID10473

N-Methylmethanamine hydrochloride

C2H8ClN

结构：CN(C)C1(C#N)CCCC1
HCID10773049

1-(Dimethylamino)cyclopentanecarbonitrile

C8H14N2

PRODUCTS

生成物

1
结构：CCC(C)(C#N)N(C)C
HCID233394

未命名化合物

收率 78%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：O
溶剂HCID962

Water

H2O

PROCEDURE

实验过程

The title compound (9.95 g, 78%) was prepared from dimethylamine hydrochloride (8.15 g, 0.1 mol), 2-butanone (8.96 ml, 0.1 mol) and potassium cyanide (6.51 g, 0.1 mol) in water (50 ml) in a similar manner to that described in D1. 1H NMR (CDCl3) δ: 1.00 (3H, t, J=7.2 Hz), 1.43 (3H, s), 1.75-1.87 (2H, m), 2.33 (6H, s).