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HRID21579

反应详情

EQUATION

反应方程式

HRID 21579 的结构方程式

REACTANTS

反应物

3
结构：CN
HCID6329

Methylamine

CH5N

结构：[NH4+].[OH-]
HCID14923

Ammonium hydroxide

H5NO

结构：COc1ccc2c(c1)c(OC(C)C)c(C(=O)O)n2C
HCID13885799

未命名化合物

PRODUCTS

生成物

1
结构：CNC(=O)c1c(OC(C)C)c2cc(OC)ccc2n1C
HCID19933216

未命名化合物

收率 45%

PROCEDURE

实验过程

Prepared from 5-methoxy-1-methyl-3-(1-methylethoxy)-1H-indole-2-carboxylic acid by the procedure of Example 1 with 40% aqueous methylamine solution substituted for ammonium hydroxide. Yield 45% after recrystallization from hexane; mp 85°-86° C.

WORKUP

后处理

  1. customYield 45% after recrystallization from hexane