HRID2163536

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID8006

1-Bromo-3-chloropropane

C3H6BrCl

HCID21584188

Chloroform methanol

C2H5Cl3O

HCID135495016

6,7-Dimethoxyquinazolin-4(1H)-one

C10H10N2O3

PRODUCTS

生成物

HCID22326631

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID6228

N,N-Dimethylformamide

C3H7NO

PROCEDURE

实验过程

1-(6,7-Dimethoxy-4-(3H)-quinazolinone-3-yl)-3-chloro-propane was prepared analogous to Example 1 (a) by reaction of 6,7-dimethoxy-4(3H)-quinazolinone with 1-bromo-3-chloro-propane in dimethyl-formamide. Rf -value (chloroform/methanol = 19/1) : 0.75.