HRID2169117

反应详情

EQUATION

反应方程式

HRID 2169117 的结构方程式

REACTANTS

反应物

2

结构：CCOC(=O)OCC

Diethyl carbonate

C5H10O3

结构：COc1cc2c(cc1OC)C(CN)C2

3,4-Dimethoxybicyclo[4.2.0]octa-1,3,5-triene-7-methanamine

C11H15NO2

PRODUCTS

生成物

1

结构：CCOC(=O)NC[C@H]1Cc2cc(OC)c(OC)cc21

Ethyl N-[[(7S)-3,4-dimethoxybicyclo[4.2.0]octa-1,3,5-trien-7-yl]methyl]carbamate

C14H19NO4

AUXILIARIES

试剂、催化剂与溶剂

1

结构：CC1CCCO1

2-Methyltetrahydrofuran

C5H10O

PROCEDURE

实验过程

5 mg of 1-(3,4-dimethoxybicyclo[4.2.0]octa-1,3,5-trien-7-yl)methanamine and 12.6 mg (10 eq) of diethyl carbonate are dissolved in 2-MeTHF.