Dimethylformamide → HCID 14235032, compound

HRID 2249192Notes

Reaction equation

HRID 2249192 reaction equation
P(Cl)(Cl)(Cl)=O.CN(C)[CH:8]=[O:9].[CH3:11][C:12]1[N:13]([CH2:18][C:19]([O:21][CH3:22])=[O:20])[C:14]([CH3:17])=[CH:15][CH:16]=1>ClCCCl>[CH3:17][C:14]1[N:13]([CH2:18][C:19]([O:21][CH3:22])=[O:20])[C:12]([CH3:11])=[CH:16][C:15]=1[CH:8]=[O:9]

Participants

5

Reactant 3

HCID 6228DimethylformamideHCID 24813Phosphorus oxychlorideHCID 1350083165766-97-4

Product 1

HCID 14235032HCID 14235032, compound

Reagents, catalysts & solvents 1

HCID 111,2-DichloroethaneSolvent

Procedure

17 ml (0.18 mol) of phosphorus oxychloride, 14 ml (0.18 mol) of anhydrous dimethylformamide and 30 g (0.18 mol) of methyl (2,5-dimethyl-pyrrol-1-yl)-acetate are reacted in 140 ml of 1,2-dichloroethane as described above.

Sources & evidence

ORD record
ord-fe84bec512df41d2ac3207779a29af1e
Source dataset
uspto-grants-1991_08
Patent number
US05043348

Reaction notes

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