HRID2269461

反应详情

EQUATION

反应方程式

HRID 2269461 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

Following a similar procedure to that described in Example (1a), 2.0 g of 4-fluoro-3-nitrophenyl 4-methoxyphenyl ketone, 2.81 g of 1-(3,4-difluorophenyl)ethylamine hydrochloride, 6.08 ml of triethylamine, 0.96 ml of titanium tetrachloride, 2.03 g of sodium cyanoborohydride and 0.62 ml of acetic acid were reacted, to obtain 2.63 g of the title compound as a yellow oil.

WORKUP

后处理

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