反应详情

150 mg 4-[3-methyl-1-(tetrahydro-pyran-2-yl)-4-(2,2,5,5-tetramethyl-piperazin-1-ylmethyl)-1H-pyrazolo[3,4-b]pyridin-6-yl]-phenol were dissolved in 10 ml of tetrahydrofurane and 0.65 ml HCl (4N in 1,4-dioxane) were added. After stirring the reaction at r.t. for 30 min the precipitated residue was isolated by filtration and washed with THF.

1. customthe reaction at r.t. for 30 min the precipitated residue
2. customwas isolated by filtration
3. washwashed with THF