HRID228536

反应详情

EQUATION

反应方程式

HRID 228536 的结构方程式

CONDITIONS

反应条件

温度
180 °C

PROCEDURE

实验过程

A mixture of 4-chloro-6,7-dimethoxyquinoline (90 mg) with 6-hydroxyquinoline (176 mg) was stirred at 180° C. for 30 min. The reaction solution was cooled to room temperature, and was then purified by column chromatography on silica gel using acetone-hexane to give the title compound (62 mg, yield 46%).

WORKUP

后处理

  1. temperatureThe reaction solution was cooled to room temperature
  2. customwas then purified by column chromatography on silica gel