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HRID2303853

反应详情

EQUATION

反应方程式

HRID 2303853 的结构方程式

REACTANTS

反应物

3
结构：[H-].[Na+]
HCID24758

Sodium hydride

HNa

结构：Cc1cc(O)cc(C)c1N
HCID76543

3,5-Dimethyl-4-aminophenol

C8H11NO

结构：CN(C(=O)OC(C)(C)C)c1cc(Cl)ccc1[N+](=O)[O-]
HCID15544598

未命名化合物

PRODUCTS

生成物

1
结构：Cc1cc(Oc2ccc([N+](=O)[O-])c(N(C)C(=O)OC(C)(C)C)c2)cc(C)c1N
HCID18184997

未命名化合物

收率 73.4%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CN(C)C=O
溶剂HCID6228

N,N-Dimethylformamide

C3H7NO

PROCEDURE

实验过程

By using 1.10 g of 4-amino-3,5-dimethylphenol, 2.29 g of t-butyl N-(5-chloro-2-nitrophenyl)-N-methylcarbamate, 0.35 g of sodium hydride (55% by weight) and 30 ml of anhydrous N,N-dimethylformamide, reaction and purification were carried out in a similar manner to that described in Reference Example 6, whereby 2.27 g of the title compound were obtained.