反应详情

In a similar manner to that described in Reference Example 6, a reaction was carried out using 2,6-di-t-butylhydroquinone (4.44 g), t-butyl N-(5-chloro-2-nitrophenyl)-N-methylcarbamate (8.60 g), sodium hydride (55 wt. %, 2.18 g) and anhydrous N,N-dimethylformamide (50 ml) and the reaction mixture was purified to give the title compound (0.60 g).

1. customthe reaction mixture was purified