Potassium Carbonate → HCID 13851593, compound

HRID 2308960Notes

Reaction equation

HRID 2308960 reaction equation
[CH3:1][O:2][C:3]1[C:8]2[CH2:9][C@@H:10]3[C@@H:15]([CH2:16][C:7]=2[CH:6]=[CH:5][CH:4]=1)[NH:14][CH2:13][CH2:12][CH2:11]3.C(=O)([O-])[O-].[K+].[K+].[CH2:23](I)[CH2:24][CH3:25]>CN(C)C=O>[CH3:1][O:2][C:3]1[C:8]2[CH2:9][C@@H:10]3[C@@H:15]([CH2:16][C:7]=2[CH:6]=[CH:5][CH:4]=1)[N:14]([CH2:23][CH2:24][CH3:25])[CH2:13][CH2:12][CH2:11]3

Participants

5

Reactant 3

HCID 11430Potassium CarbonateHCID 336431-IodopropaneHCID 13851586HCID 13851586, compound

Product 1

HCID 13851593HCID 13851593, compound

Reagents, catalysts & solvents 1

HCID 6228DimethylformamideSolvent

Procedure

3 g of trans-1,2,3,4,4a,5,10,10a-octahydro-6-methoxybenzo[g]quinoline are dissolved in 100 ml of dimethylformamide. 3.8 g potassium carbonate and 1.8 ml of n-propyl iodide are subsequently added and the obtained suspension is stirred for 2 days at room temperature.

Sources & evidence

ORD record
ord-3f3d4187239542b6a5db85533d0ea089
Source dataset
uspto-grants-1987_09
Patent number
US04692453

Reaction notes

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